GCMS analysis results for unknown compounds, sample AE10199, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \MSDCHEM\1\DATA\050802\10199.D Vial: 17 Acq On 9 May 2002 4:27 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Misc : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Antipyrine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.43 ug/L 530997 Phenanthranene-dl 0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Antipyrine 188 C11H12N2O 000060-80-0 50 2 Antipyrine 188 C11H12N2O 000060-80-0 50 3 Antipyrine 188 C11H12N2O 000060-80 50 4 Phenanthrene-dlO 188 C14D10 001517-22 -2 47 Abundance Scan 3409 (23.109 min): 10199.D (-3403) (-) m/z 188 10/100008 188

5000

94 1 I [ I 17 III1111I I 1 I I < k [ 80 160 22.80 23.00 23.20 23.40 40 49 57 66 Ot 1 r ’ ■1 r , ! ! | U h A| !II, p.II |. ." /। | ...................................... i i | i t i i | i I I i | I i i | | i । । । | I r i i | i i I | | । | i i | | i 11. m/z 94.05 20.54% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79725: Antipyrine 188 96 1 ........ /......................... । । । ~। । । y । i t i । । i-1 । | । । । । [ 5000 77 22.80 23.00 23.20 23.40 56 m/z 184.10 16.97% 105 27 39 67 I, 115 130 145 159 173 i 0 TTTTTTT ! I l‘p I I ", 3 TH— 'i । rlli p 1‘Hl‘i । । +Hl । । । rt'r । ['i । tl । m*I*‘n । । । । । 111 । । i’j mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125688: Antipyrine 188 96 ■ ■ । ■ 1 1 i 1 1 1 1 i 1 1 1 1 1 22.80 23.00 23.20 23.40 5000 77 m/z 80.10 12.40% 56 1 105 39 27 64 ill | 115 129 145 159 173 01 T-p-r Aosim—* 1 | dVI'i nil I'l , . /I1! h । Nlrr i H -TTl’l i i i । I I'l i । i I I l' I > > I I I I I I I I I I TuTrp m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 , I I I I I y I I. I I I I I > I I I I I I I" Abundance #125690: Antipyrine 188 22.80 23.00 23.20 23.40 m/z 189.15 12.25% 96 A 5000 77 56 105 43 69 115 129 159 173 । 0 I i | f I r i [ i I I I [ i i i —l 85. 4 I, al.-Ptr r। i । । i । । । i । | i i । । । । I < i । । i । ...... 1...................... 1 t I I I I I I I I I I I I • I j I I PfT

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10199.D 050102.M Thu May 09 13:36:03 2002 Page 8

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