GCMS calibration table for TCLP analysis, April 2002

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Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.

NYC-WTC_000044748–000044755

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2202\8756 .D Vial: 12 Acq On : 22 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Pyridine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.86 0.44 ug/1 58340 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyridine 79 C5H5N 000110-86-1 91 2 Cyclobutane, 1,2-bis(methylene)- 80 C6H8 014296-80-1-64 3 Pyridine, compd. with sulfur trioxi 159 C5H5NO3S: 026412-87-3 64 4 2-Pyridinecarboxylic acid 123 C6H5NO2 000098-98-6 33 Abundance Scan 89 (5.860 min): 8756.D (-) m/z 78.95 100.00% 79

52 5000

1 1 1 ' i 1 ' ‘ ' i ' ' ' i ' ■ ' ' i 1 1 1 2 39 . 49 5.60 5.80 6.00 6.20 30, 11. —44 7 , 84 11111111 Ttlf I l1 ' ■' i •1 1 11 ■1 m/ Z 52.00 58.00% m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62631: Pyridine 79 52

5000 1 1 1 ' it ' I 5.60) 5.80 6.00 6.20 m/z !50.95 28.86% 26 38 49

U_ I i । । i ( । । I I । i *Im । । I I । । । । । । । । । rd ■ 1.............. 75 | ' | । । 11 | । । । ' | । । 11 | I i I i | i i | | | I I I I | 1 I I I | I TT

m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #437: Cyclobutane, 1,2-bis(methylene)- 79 1 1 I ' ' ‘ ' |tt ■ 1 । ■ ■ ■ ' । 1 ‘ ' 52 5.601 5.80 6.00 6.20 5000 39 m/ z !50.00 24.21%

m/z-> 15 I I I t I I I I I I 1

20 25 > ■ । ■ ■ ■ ■ i ■ I ■

30 35 49 i 1 1 1 1 i ■ ' '1 40 45 50 155. 6062565... i 70 75 80 85 90 Abundance #12123: Pyridine, compd. with sulfur trioxide (1:1) 1 ■ 1 1 ' ' ‘ I , Mw AA/ ’ I I I I I 1 1 I I I I

52 79 m/z 5.60 5.80 77.95 6.00 13.46% 6.20

5000

48 64 26 i1 1 ■' i'1 1 11 1 । । । i" । T"gi"i mp-eTi r 44 + -— 60 76 | ' । । । 1 ‘ । । 1 ' । 1 > > ‘ i ‘ 1 1 ' i 1 I kk ' ' ' i 1 1 ' ■ i 1 1 m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5.60 5.80 6.00 6.20

8756.D GCMS0412.M Tue Apr 23 08:21:48 2002 Page 1

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