GCMS Sample AE03386 Report, March 12 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2102\3386.D Vial: 48 Acq On : 23 Feb 2002 3:24 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Pyrene Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

30.81 3.65 ug/1 237929 Chrysene-dl2 33.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrene 202 C16H10 000129-00-0 83 2 Fluoranthene 202 C16H10 000206-44-0 64 3 4-Morpholineacetonitrile, .alpha.-p 202 C12H14N20 015190-10-0 9 4 Pyrimidine, 4-methoxy-6-(2-hydroxyp 202 C11H10N2O2 097630-79-0 5 Abundance Scan 2807 (30.813 min): 3386.D (-) m/z 234 .95 100.00% 2. 6

■165 5000-

199 .................................................

m/z-> Abundance 75 00 +38.51,4+4444114123137151 1248 320 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Xx... #69819: Pyrene “ in 1 1 1 1 ' ' ■ I " " I " " | " 30.40 30.60 30.80 31.00 31.20 m/ z 236.95 64.86%

202

5000 30.40 30.60 30.80 31.00 31.20 101 m/ z 165.10 56.59% 62 88 150 174 . . ■ i . . ■ . i . . . . । ■ ril i' ' ' i ' ' ' ■ i 1 1 1 ' i 1 1 1 ' I 1 1 ' 11 1 1 1 1 1 1 1 m/Z->. 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 202

30.40 30.60 30.80 31.00 31.20 5000- m/z 198.95 18.99% on 00 101 150 174 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #69793: 4-Morpholineacetonitrile, alpha.-pheny- ,........ 116 202 30.40 30.60 30.80 31.00 31.20 86 171 m/ z 236.05 15.02% 5000- 56

I 157 “ | ' A | | । । I I | I I I I | ! I ! I | I I ! I | I I ......... / (.......... ‘ I’’ I ' ' 1 ' 1 1 ' 1 ' I 11 1'111 11 111 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00 31.20

3386.D GCMS0208.M Tue Mar 12 12:29:37 2002 Page 1

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