GCMS Sample AE03386 Report, March 12 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB2102\3386.D Vial: 48 Acq On : 23 Feb 2002 3:24 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Fluoranthene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

30.81 3.65 ug/1 237929 Chrysene-dl2 33.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Fluoranthene 202 C16H10 000206-44-0 86 2 Pyrene 202 C16H10 000129-00-0 86 3 Benzaldehyde, 2,6-difuloro-3,4-dime 202 C9H8F2O3 000000-00-0 9 4 Benzene, 1,1'-(1,3-butadiyne-1,4-di 202 C16H10 000886-66-8 7 Abundance Scan 2807 (30.813 min): 3386.D (-) ] m/ z 234.95 100. 00% 2: 5 ! 165 5000

199 ........ s......... ,38,51..7 32191.122127151,177P 1248, 178 1 212 320 " I " " I " "'I " 30.40 30.60 30.80 31.00 31.20 m/z 236.95 64.86% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #69814: Fluoranthene 202

5000 30.40 30.60 30.80 31.00 31.20 101 m/z165 .To 56.59% 88 150 174 ——————— ' l' ' ' ' i ' 1 ' ' i ' ' ' ■ i ' ' ' 11 ' ' ■' i1 ' ' ' i '' 1 1 1 1 1 1 ' I 1 1 ' 1 I । 1 1 । I 1 ' '1 1 ' 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 202 ............. M................. 30.40 30.60 30.80 31.00 31.20 5000 m/z 198.95 18.99% 101 88 150 174 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #23220: Benzaldehyde, 2,6-difuloro-3,4-dimethoxy- 202 30.40 30.60 30.80 31.00 31.20 m/ z 23 6.05 15.02% 5000 187 83> 115 101 131 m/z-> 44 159 111111111111111111‘11—1TT—1110111119—91—3OITTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 .... /M..... 30.40 30.60 30.80 31.00 31.20

3386.D GCMS0208.M Tue Mar 12 12:28:14 2002 Page 1

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