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GCMS blank results for sample AD29022, Dec 17 2001

Machine-extracted title · confidence 95%

Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.

NYC-WTC_000035776–000035787

Folder label: “GCMS X 11/30/01 A 12/10/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1001\LB.D Vial: 3 Acq On : 10 Dec 2001 11:42 am Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 303 rBV 311068 907560 13.84% 2.573% 2 11.349 683 687 692 rBV 65937 154130 2.35% 0.437% 3 11.422 692 695 709 rVB 71082 209467 3.19% 0.594% 4 11.670 716 722 739 rBV 1900056 4745136 72.35% 13.451% 5 15.278 1109 1115 1133 rBV 2801001 6023133 91.83% 17.073%

6 20.557 1683 1690 1709 rBV 2895588 6558878 100.00% 18.592% 7 22.677 1916 1921 1929 rBV2 23611 90115 1.37% 0.255% 8 23.247 1978 1983 1990 rBV3 17086 66909 1.02% 0.190% 9 24.973 2164 2171 2183 rBV2 2766109 6090868 92.86% 17.265% 10 25.119 2183 2187 2196 rVB2 26251 78454 1.20% 0.222%

11 26.983 2385 2390 2401 rBV 366501 721205 11.00% 2.044% 12 30.049 2719 2724 2732 rBV 384994 786108 11.99% 2.228% 13 30.288 2744 2750 2759 rBV 429270 887624 13.53% 2.516% 14 33.005 3038 3046 3065 rBV2 1817977 4297181 65.52% 12.181% 15 33.290 3072 3077 3088 rVB2 44326 118342 1.80% 0.335%

16 35.787 3344 3349 3357 rBV 36987 95572 1.46% 0.271% 17 37.100 3484 3492 3510 rBV2 1212690 3447794 52.57% 9.773%

Sum of corrected areas: 35278476

LB.D GCMS1126.M Thu Dec 13 10:54:50 2001

NYC-WTC_000035780

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NYC-WTC_000035780Source: NYC Law Department, mirrored locally

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