Laboratory analysis report for sample AD29285 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036311–000036324Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
Data File : C:\HPCHEM\l\DATA\DEC1201\29293.D Vial: 14 Acq On 12 Dec 2001 3:40 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.597 274 278 291 rBV 413493 1026293 14.29% 2.721% 2 7.744 291 294 308 rVB 41027 146242 2.04% 0.388% 3 11.342 682 686 691 rBV 93561 202563 2.82% 0.537% 4 11.425 691 695 713 rW 98383 283477 3.95% 0.751% 5 11.673 715 722 746 rBV 2108935 5307882 73.92% 14.071%
6 15.271 1109 1114 1132 rBV 2969166 6587958 91.75% 17.464% . 7 20.550 1683 1689 1713 rBV 3245651 7180375 100.00% 19.035% 8 24.975 2164 2171 2183 rBV2 2975038 6697469 93.27% 17.755% 9 25.122 2183 2187 2193 rVB 25450 74222 1.03% 0.197% 10 26.985 2385 2390 2396 rBV 45489 91214 1.27% 0.242%
11 30.052 2718 2724 2731 rBV 481482 976569 13.60% 2.589% 12 33.008 3039 3046 3070 rBV2 2121758 5038291 70.17% 13.356% 13 33.292 3072 3077 3088 rVB 37996 116755 1.63% 0.310% 14 35.027 3261 3266 3276 rBV 22083 72478 1.01% 0.192% 15 37.102 3484 3492 3509 rBV2 1339724 3920803 54.60% 10.394%
Sum of corrected areas: 37722591
29293.D GCMS1126.M Fri Dec 28 15:24:09 2001
NYC-WTC_000036316
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NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036137
Laboratory report noting GCMS scan results for sample AD29233 with phthalates and nonadecanol detected.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037314
Gas chromatography-mass spectrometry report documenting analysis of sample AD30011 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037255
Gas chromatography-mass spectrometry report documenting analysis of sample AD30013 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035931
Laboratory report noting detection of Decanedioic acid bis(2-Ethylhexyl) ester in sample AD29027 on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder