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GCMS analysis comments, sample AD29233, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report noting GCMS scan results for sample AD29233 with phthalates and nonadecanol detected.

NYC-WTC_000036137–000036150

Folder label: “GCMS X 12/3/01 A 12/10/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC1001\29233.D Vial: 15 Acq On : 11 Dec 2001 12:23 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 290 rBV 474998 1134654 16.36% 2.869% 2 7.741 290 294 309 rVB 69554 235995 3.40% 0.597% 3 9.219 451 455 467 rBV 60260 216970 3.13% 0.549% 4 11.331 681 685 690 rBV 457949 915180 13.20% 2.314% 5 11.413 690 694 714 rVB 455343 1139482 16.43% 2.882%

6 11.670 714 722 740 rBV2 2159216 6118412 88.23% 15.472% 7 15.278 1109 1115 1131 rBV 2922814 6399172 92.28% 16.182% 8 20.548 1683 1689 1707 rBV 3068782 6934628 100.00% 17.536% 9 24.973 2164 2171 2183 rBV2 2949661 6496463 93.68% 16.428% 10 25.120 2183 2187 2197 rVB 26588 83241 1.20% 0.210% 11 29.664 2675 2682 2694 rBV 92981 222480 3.21% 0.563% 12 30.049 2717 2724 2733 rBV 437264 885751 12.77% 2.240% 13 33.005 3038 3046 3061 rBV2 2063146 4804098 69.28% 12.149% 14 33.290 3071 3077 3084 rBV 39686 102513 1.48% 0.259% 15 37.100 3483 3492 3518 rBV2 1364334 3855455 55.60% 9.750%

Sum of corrected areas: 39544494

29233.D GCMS1126.M Fri Dec 14 16:12:32 2001

NYC-WTC_000036142

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NYC-WTC_000036142Source: NYC Law Department, mirrored locally

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