Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
NYC-WTC_000036220–000036231Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
Data File : C:\HPCHEM\1\DATA\DEC1001\29291.D Vial: 11 Acq On : 12 Dec 2001 9:29 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.603 275 279 290 rBV 289328 750296 11.57% 2.181% 2 7.741 292 294 311 rVB 37643 144708 2.23% 0.421% 3 11.340 682 686 691 rBV 139127 306861 4.73% 0.892% 4 11.422 691 695 714 rVB 148299 424703 6.55% 1.234% 5 11.670 714 722 746 rBV2 1826035 5192779 80.08% 15.094%
6 15.278 1109 1115 1135 rBV 2766245 5983106 92.26% 17.391% 7 20.557 1683 1690 1709 rBV 2893374 6484760 100.00% 18.849% 8 24.972 2165 2171 2183 rBV2 2796404 5975623 92.15% 17.370% 9 25.119 2184 2187 2196 rVB 23895 72790 1.12% 0.212% 10 26.983 2386 2390 2402 rVB 40252 90001 1.39% 0.262%
11 30.049 2718 2724 2736 rBV 461023 929193 14.33% 2.701% 12 33.005 3040 3046 3066 rBV2 1910502 4447062 68.58% 12.926% 13 37.099 3484 3492 3511 rBV 1227782 3600963 55.53% 10.467%
Sum of corrected areas: 34402845
29291.D GCMS1126.M Wed Dec 19 12:54:05 2001
NYC-WTC_000036225
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NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder