Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
NYC-WTC_000036114–000036125Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
* Data File : C:\HPCHEM\1\DATA\DEC1001\29230.D Vial: 18 Acq On : 11 Dec 2001 3:18 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total
1 7.598 274 278 290 rBV 388271 961373 14.48% 2.675% 2 7.745 291 294 309 rVB 40966 151995 2.29% 0.423% 3 11.334 681 685 690 rBV 325711 669867 10.09% 1.864% 4 11.417 690 694 713 rVB 331399 872957 13.14% 2.429% 5 11.674 713 722 745 rBV2 1994110 5795249 87.26% 16.124%
6 15.273 1109 1114 1133 rBV 2796903 6098612 91.83% 16.968% 7 20.551 1682 1689 1711 rBV 3055060 6641503 100.00% 18.478% 8 24.976 2164 2171 2183 rBV2 2613569 6061486 91.27% 16.864% 9 25.123 2183 2187 2207 rVB2 25849 97293 1.46% 0.271% 10 30.053 2718 2724 2731 rBV 390413 795548 11.98% 2.213%
11 33.009 3039 3046 3064 rBV 1821957 4286438 64.54% 11.926% 12 33.294 3072 3077 3087 rVB 24729 68536 1.03% 0.191% 13 37.094 3484 3491 3510 rBV2 1197344 3441517 51.82% 9.575%
Sum of corrected areas: 35942374
29230.D GCMS1126.M Fri Dec 14 16:08:37 2001
NYC-WTC_000036119
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NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017796
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30354 conducted on January 10, 2002.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder