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GCMS analysis comments, sample AD29234, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.

NYC-WTC_000036092–000036102

Folder label: “GCMS X 12/3/01 A 12/10/01

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Scanned page image, NYC-WTC_000036097
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\l\DATA\DEC1001\29189.D Vial: 20 Acq On : 11 Dec 2001 5:15 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.594 274 278 301 rBV 300765 852959 14.34% 2.788% 2 11.339 683 686 692 rBV 71815 172936 2.91% 0.565% 3 11.422 692 695 710 rVB 83859 233859 3.93% 0.765% 4 11.670 715 722 746 rBV 1750167 4368480 73.46% 14.281% 5 15.278 1109 1115 1133 rBV 2454356 5409780 90.97% 17.685%

6 20.547 1683 1689 1712 rBV 2646156 5947012 100.00% 19.442% 7 24.972 2165 2171 2183 rBV2 2461297 5452753 91.69% 17.826% 8 25.119 2183 2187 2195 rVB 23552 75627 1.27% 0.247% 9 26.992 2386 2391 2396 rBV 143221 293300 4.93% 0.959% 10 30.049 2719 2724 2731 rBV 337505 701356 11.79% 2.293%

11 33.005 3040 3046 3055 rBV2 1755264 4025198 67.68% 13.159% 12 33.289 3073 3077 3089 rVB 24689 75235 1.27% 0.246% 13 37.099 3484 3492 3507 rBV2 1022843 2980738 50.12% 9.744%

Sum of corrected areas: 30589233

29189.D GCMS1126.M Fri Dec 14 16:07:20 2001

NYC-WTC_000036097

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NYC-WTC_000036097Source: NYC Law Department, mirrored locally

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