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GCMS analysis results for sample AD30353, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30353 conducted on January 10, 2002.

NYC-WTC_000017692–000017702

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

"Data File : C:\HPCHEM\1\DATA\DEC2701\30353.D Vial: 17 Acq On : 28 Dec 2001 3:42 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.613 276 280 294 rBV 530545 1402324 14.62% 2.797% 2 11.349 684 687 693 rBV 88063 216086 2.25% 0.431% 3 11.432 693 696 717 rVB 96820 330638 3.45% 0.660% 4 11.680 717 723 752 rBV 2687937 7308767 76.19% 14.580% 5 14.306 1005 1009 1015 rVB 59480 124447 1.30% 0.248%

6 15.279 1109 1115 1134 rBV 3674928 8723128 90.94% 17.401% 7 17.454 1346 1352 1359 rBV2 58676 133348 1.39% 0.266% 8 20.557 1684 1690 1716 rBV 4087063 9592520 100.00% 19.136% 9 24.982 2165 2172 2205 rBV2 3423671 8939236 93.19% 17.832% 10 27.002 2387 2392 2403 rBV 83923 237663 2.48% 0.474%'

11 30.059 2719 2725 2738 rBV 554407 1210029 12.61% 2.414% 12 33.024 3039 3048 3074 rBV2 2527733 6622484 69.04% 13.211% 13 37.119 3484 3494 3520 rBV2 1666314 5288575 55.13% 10.550%

Sum of corrected areas: 50129245

30353.D GCMS1126.M Wed Jan 02 10:52:21 2002

NYC-WTC_000017697

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NYC-WTC_000017697Source: NYC Law Department, mirrored locally

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