Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
NYC-WTC_000036079–000036091Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
‘Data File : C:\HPCHEM\1\DATA\DEC1001\29234.D Vial: 23 Acq On : 11 Dec 2001 8:10 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.599 273 278 290 rBV 354175 907658 14.53% 2.470% 2 7.737 291 293 310 rVB2 29774 117625 1.88% 0.320% 3 9.215 450 454 469 rBV 70484 254003 4.07% 0.691% 4 11.326 680 684 689 rBV 560860 1108676 17.75% 3.017% 5 11.409 689 693 712 rVB 583996 1416598 22.68% 3.855%
6 11.629 712 717 718 rBV 643750 1069913 17.13% 2.912% 7 11.666 718 721 744 rVB 1923652 5005426 80.12% 13.623% 8 15.274 1108 1114 1132 rBV 2746365 5877696 94.09% 15.997% 9 20.553 1682 1689 1710 rBV 2777178 6247218 100.00% 17.003% 10 24.968 2164 2170 2183 TBV2 2659647 5968700 95.54% 16.245%
11 25.115 2183 2186 2198 rVB 23090 75035 1.20% 0.204% 12 30.054 2718 2724 2730 rBV 302011 634415 10.16% 1.727% 13 33.010 3039 3046 3059 rBV2 1803953 4448005 71.20% 12.106% 14 37.096 3483 3491 3511 rBV2 1239013 3611580 57.81% 9.829%
Sum of corrected areas: 36742548
29234.D GCMS1126.M Fri Dec 14 16:48:14 2001
NYC-WTC_000036084
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NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder