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GCMS analysis comments, sample AD29028, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in sample AD29028 analyzed on December 18, 2001.

NYC-WTC_000035990–000035999

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\1\DATA\DEC1001\29028.D Vial: 32 Acq On : 11 Dec 2001 6:55 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan.scan scan TY height area % max. total

1 7.606 275 279 291 rBV 363527 906263 11.60% 2.266% 2 7.744 291 294 314 rVB 41137 165529 2.12% 0.414% 3 11.352 684 687 692 rBV 32469 81816 1.05% 0.205% 4 11.434 692 696 704 rW 35226 94565 1.21% 0.236% 5 11.673 717 722 745 rBV 2167854 5424689 69.46% 13.563%

6 15.272 1109 1114 1132 rBV 3153066 7065657 90.47% 17.665% 7 20.550 1683 1689 1711 rBV 3582846 7810343 100.00% 19.527% 8 24.975 2164 2171 2184 rBV2 3372010 7250358 92.83% 18.127% 9 25.122 2184 2187 2196 rVB2 27327 78480 1.00% 0.196% 10 30.052 2718 2724 2732 rBV 458335 932106 11.93% 2.330%

11 33.008 3037 3046 3064 rBV2 2333974 5564879 71.25% 13.913% 12 33.293 3071 3077 3085 rBV2 39459 101251 1.30% 0.253% 13 37.103 3484 3492 3512 rBV2 1598837 4520997 57.88% 11.303%

Sum of corrected areas: 39996933

29028.D GCMS1126.M Wed Dec 12 15:49:18 2001

NYC-WTC_000035995

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NYC-WTC_000035995Source: NYC Law Department, mirrored locally

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