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GCMS analysis comments, sample AD29027, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting detection of Decanedioic acid bis(2-Ethylhexyl) ester in sample AD29027 on December 18, 2001.

NYC-WTC_000035931–000035943

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File : C:\HPCHEM\1\DATA\DEC1001\29027.D Vial: 28 Acq On : 11 Dec 2001 3:01 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.607 274 279 290 rBV 354789 912494 10.72% 2.062% 2 7.745 292 294 317 rVB 35885 144390 1.70% 0.326% 3 11.344 683 686 691 rBV 59556 141179 1.66% 0.319% 4 11.426 691 695 704 rVB 68596 176458 2.07% 0.399% 5 11.674 716 722 741 rBV 2450623 6156985 72.32% 13.916%

6 15.273 1109 1114 1133 rBV 3490173 7776915 91.35% 17.578% 7 20.552 1683 1689 1708 rBV 3829928 8513717 100.00% 19.243% 8 24.977 2164 2171 2182 rBV2 3597221 7963527 93.54% 18.000% 9 25.123 2183 2187 2198 rVB 34158 109417 1.29% 0.247% 10 30.053 2716 2724 2733 rBV 414095 844470 9.92% 1.909%

11 33.009 3039 3046 3067 rBV2 2553789 6269435 73.64% 14.171% 12 35.561 3319 3324 3337 rBV 65904 231335 2.72% 0.523% 13 37.104 3484 3492 3513 rBV2 1771899 5002408 58.76% 11.307%

Sum of corrected areas: 44242730

29027.D GCMS1126.M Wed Dec 12 15:48:02 2001

NYC-WTC_000035936

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NYC-WTC_000035936Source: NYC Law Department, mirrored locally

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