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GCMS analysis results sample AD29460, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29460 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036458–000036468

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File : C:\HPCHEM\1\DATA\DEC1201\29460.D Vial: 19 Acq On : 12 Dec 2001 8:33 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 274 278 299 rBV 328549 930378 12.88% 2.473% 2 9.233 452 456 473 rBV2 23356 106090 1.47% 0.282% 3 11.335 681 685 690 rBV 132045 282894 3.91% 0.752% 4 11.418 690 694 714 rVB 140780 408597 5.65% 1.086% 5 11.666 714 721 745 rBV 2056750 5648018 78.16% 15.011%

6 15.274 1108 1114 1132 rBV 3114250 6798716 94.08% 18.. 069% 7 20.552 1683 1689 1705 rBV 3341949 7226183 100.00% 19.205% 8 24.968 2164 2170 2183 rBV2 2980195 6719503 92.99% 17.858% 9 25.115 2183 2186 2193 rVB2 23377 74377 1.03% 0.198% 10 30.045 2718 2723 2733 rBV 391151 823010 11.39% 2.187%

11 33.010 3039 3046 3063 rBV2 2021253 4844077 67.04% 12.874% 12 33.285 .3071 3076 3087 rVB 25992 77476 1.07% 0.206% 13 37.095 3483 3491 3508 rBV2 1308754 3687125 51.02% 9.799%

Sum of corrected areas: 37626444

29460 .D GCMS1126.M Fri Dec 21 12:27:16 2001

NYC-WTC_000036463

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NYC-WTC_000036463Source: NYC Law Department, mirrored locally

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