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GCMS analysis comments for sample AD29190, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29190 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.

NYC-WTC_000035843–000035852

Folder label: “GCMS X 11/30/01 A 12/10/01

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29190.D Vial: 12 Acq On : 10 Dec 2001 9:28 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.598 274 278 315 rVB 398491 1132840 14.99% 2.972% 2 11.436 692 696 706 rVB 32734 98134 1.30% 0.257% 3 11.674 716 722 746 rBV 2079013 5296498 70.09% 13.894% 4 15.273 1108 1114 1132 rBV 3186190 6877775 91.02% 18.042% 5 20.552 1683 1689 1711 rBV 3470343 7556566 100.00% 19.823%

6 24.977 2164 2171 2182 rBV2 3012189 6922990 91.62% 18.161% 7 25.123 2183 2187 2197 rVB 25429 80096 1.06% 0.210% 8 26.987 2383 2390 2396 rBV 46768 99126 1.31% 0.260% 9 30.044 2718 2723 2732 rBV 430523 910204 12.05% 2.388% 10 33.009 3039 3046 3062 rBV2 2085188 4955113 65.57% 12.999%

11 35.571 3319 3325 3338 rBV 65037 222988 2.95% 0.585% 12 37.095 3484 3491 3514 rBV2 1335211 3967532 52.50% 10.408%

Sum of corrected areas: 38119862

29190.D GCMS1126.M Wed Dec 12 16:10:08 2001

NYC-WTC_000035848

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NYC-WTC_000035848Source: NYC Law Department, mirrored locally

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