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GCMS analysis comments for sample AD29024, Dec 18 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29024 indicate detection of bis(2-Ethylhexyl)phthalate and no unusual compounds.

NYC-WTC_000035909–000035918

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29024.D Vial: 31 Acq On : 11 Dec 2001 5:56 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 274 278 291 rBV 292572 809460 10.58% 2.098% 2 7.736 291 293 313 rVB 31674 134453 1.76% 0.349% 3 11.436 692 696 709 rVB 26873 91954 1.20% 0.238% 4 11.675 716 722 746 rBV 2010649 5443043 71.13% 14.110% 5 15.273 1109 1114 1132 rBV 3255397 7053921 92.18% 18.285%

6 20.552 1683 1689 1706 rBV 3479411 7652457 100.00% 19.837% 7 24.977 2164 2171 2183 rBV2 3146308 7050312 92.13% 18.276% 8 25.124 2183 2187 2201 rVB 28838 96567 1.26% 0.250% 9 30.054 2718 2724 2735 rBV 356756 742066 9.70% 1.924% 10 33.010 3039 3046 3068 rBV2 2244690 5215014 68.15% 13.518% 11 33.294 3071 3077 3091 rVB 58793 176762 2.31% 0.458% 12 37.104 3484 3492 3508 rBV 1440165 4111000 53.72% 10.657%

Sum of corrected areas: 38577009 29024.D GCMS1126.M Wed Dec 12 15:44:00 2001

NYC-WTC_000035914

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NYC-WTC_000035914Source: NYC Law Department, mirrored locally

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