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Document / 11 pages

GCMS analysis comments, sample AD29140, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting GCMS scan results for sample AD29140 with one compound recovery outside acceptance range.

NYC-WTC_000036029–000036039

Folder label: “GCMS X 11/30/01 A 12/11/01

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Scanned page image, NYC-WTC_000036034
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29140.D Vial: 37 Acq On : 11 Dec 2001 11:46 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method 4 C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 292 rBV 307391 784888 10.04% 2.011% 2 7.750 292 295 312 rVB 32442 130462 1.67% 0.334% 3 11.348 684 687 693 rBV 40265 99949 1.28% 0.256% 4 11.431 693 696 717 rVB 45780 146592 1.87% 0.376% 5 11.670 717 722 741 rBV 2197589 5520856 70.61% 14.146%

6 15.277 1109 1115 1133 rBV 3249912 7050898 90.17% 18.067% 7 20.556 1683 1690 1707 rBV 3485357 7819246 100.00% 20.035% 8 24.972 2165 2171 2183 rBV2 3136672 7087124 90.64% 18.159% 9 30.049 2719 2724 2734 rVB 404873 814269 10.41% 2.086% 10 33.005 3039 3046 3068 rBV2 2160117 5289366 67.65% 13.553%

11 37.099 3484 3492 3511 rBV2 1501918 4283605 54.78% 10.976%

Sum of corrected areas: 39027255

29140.D GCMS1126.M Fri Dec 21 15:07:27 2001

NYC-WTC_000036034

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NYC-WTC_000036034Source: NYC Law Department, mirrored locally

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