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GCMS analysis comments, sample AD29025, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.

NYC-WTC_000035919–000035930

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

- Data File : C:\HPCHEM\l\DATA\DEC1001\29025.D Vial: 29 Acq On : 11 Dec 2001 3:59 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.606 274 279 290 rBV 275730 735414 10.06% 1.924% 2 7.744 291 294 310 rVB 36071 136959 1.87% 0.358% 3 11.343 682 686 691 rBV 70080 160601 2.20% 0.420% 4 11.425 691 695 710 rVB 81562 241356 3.30% 0.632% 5 11.673 716 722 745 rBV 2096664 5417746 74.15% 14.175%

6 15.272 1109 1114 1133 rBV 3023120 6864621 93.95% 17.961% 7 20.551 1683 1689 1701 rBV 3321214 7306830 100.00% 19.118% 8 24.975 2164 2171 2183 rBV2 3101321 6872063 94.05% 17.981% 9 25.113 2183 2186 2194 rVB2 25704 77119 1.06% 0.202% 10 26.986 2385 2390 2397 rBV 43533 89727 1.23% 0.235%

11 30.052 2718 2724 2732 rBV 368115 728044 9.96% 1.905% 12 33.008 3038 3046 3070 rBV2 2316468 5333529 72.99% 13.955% 13 37.103 3484 3492 3509 rBV2 1486833 4255081 58.23% 11.133%

Sum of corrected areas: 38219090

29025.D GCMS1126.M Wed Dec 12 15:45:08 2001

NYC-WTC_000035924

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NYC-WTC_000035924Source: NYC Law Department, mirrored locally

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