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GCMS analysis comments for sample AD29141, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.

NYC-WTC_000035831–000035842

Folder label: “GCMS X 11/30/01 A 12/10/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29141.D Vial: 8 Acq On : 10 Dec 2001 5:34 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.600 274 278 291 rBV 405894 1067867 15.79% 3.068% 2 7.747 291 294 311 rVB2 49236 191728 2.84% 0.551% 3 11.346 683 686 691 rBV 46532 111731 1.65% 0.321% 4 11.428 691 695 711 rVB 57682 177905 2.63% 0.511% 5 11.676 715 722 741 rBV 1774214 4818374 71.25% 13.842%

6 15.275 1108 1114 1126 rBV 2882075 6086397 90.00% 17.485% 7 20.554 1683 1689 1710 rBV 3147385 6762583 100.00% 19.427% 8 24.969 2164 2170 2183 rBV2 2744602 6229428 92.12% 17.896% 9 25.116 2183 2186 2195 rVB 23925 69774 1.03% 0.200% 10 30.046 2718 2723 2731 rBV 436824 928413 13.73% 2.667%

11 33.011 3039 3046 3061 rBV2 1854974 4549813 67.28% 13.071% 12 33.287 3071 3076 3085 rBV 56321 140237 2.07% 0.403% 13 37.097 3483 3491 3504 rBV2 1327336 3675144 54.35% 10.558%

Sum of corrected areas: 34809394

29141.D GCMS1126.M Wed Dec 12 16:08:09 2001

NYC-WTC_000035836

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NYC-WTC_000035836Source: NYC Law Department, mirrored locally

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