Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036243–000036254Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
Data File : C:\HPCHEM\l\DATA\DEC1001\29294.D Vial: 10 Acq On 12 Dec 2001 8:30 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.596 274 278 291 rBV 333333 863551 12.88% 2.552% 2 7.743 291 294 311 rVB 44056 161833 2.41% 0.478% 3 11.341 682 686 692 rBV 67930 166712 2.49% 0.493% 4 11.424 692 695 715 rVB 77424 245443 3.66% 0.725% 5 11.672 715 722 745 rBV 1973718 4987549 74.38% 14.740%
6 15.270 1109 1114 1134 rBV 2751164 6238936 93.04% 18.439% 7 20.549 1683 1689 1713 rBV 3007841 6705608 100.00% 19.818% 8 24.974 2164 2171 2183 rBV2 2751532 6053255 90.27% 17.890% 9 25.121 2183 2187 2196 rVB2 22169 76871 1.15% 0.227% 10 26.985 2386 2390 2399 rBV 30830 67332 1.00% 0.199%
11 30.051 2718 2724 2731 rBV 333140 666204 9.94% 1.969% 12 33.007 3039 3046 3063 rBV2 1847383 4333882 64.63% 12.808% 13 37.101 3484 3492 3510 rBV2 1126500 3269268 48.75% 9.662%
Sum of corrected areas: 33836444
29294.D GCMS1126.M Wed Dec 19 12:55:27 2001
NYC-WTC_000036248
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NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder