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GCMS sample analysis AD29295, Dec 2001

Machine-extracted title · confidence 95%

Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.

NYC-WTC_000036267–000036277

Folder label: “GCMS X 12/4/01 A 12/10/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29296.D Vial: 9 Acq On 12 Dec 2001 7:32 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 312 rBV 445464 1288187 17.62% 3.368% 2 11.340 682 686 691 rBV 134396 285053 3.90% 0.745% 3 11.422 691 695 714 rVB 139621 397341 5.44% 1.039% 4 11.670 714 722 746 rBV2 2138745 5732863 78.43% 14.990% 5 15.278 1109 1115 1133 rBV 2978516 6772424 92.65% 17.709%

6 20.548 1683 1689 1706 rBV 3266734 7309837 100.00% 19.114% 7 24.973 2164 2171 2184 rBV2 3123217 6729360 92.06% 17.596% 8 26.992 2386 2391 2399 rBV 37892 84270 1.15% 0.220% 9 30.049 2719 2724 2733 rBV 449016 891479 12.20% 2.331% 10 33.005 3039 3046 3062 rBV2 2111450 4910335 67.17% 12.840%

11 37.100 3484 3492 3516 rBV 1336863 3842637 52.57% 10.048%

Sum of corrected areas: 38243786

29296.D GCMS1126.M Wed Dec 19 12:58:04 2001

NYC-WTC_000036272

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NYC-WTC_000036272Source: NYC Law Department, mirrored locally

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