Laboratory notes indicating re-extraction is required due to low recovery and potential contamination.
NYC-WTC_000035745–000035754Folder label: “GCMS X 11/28/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
Data File C:\HPCHEM\1\DATA\DEC0 601\28861.D Vial: 37 Acq On 7 Dec 2001 10:49 am Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.612 276 280 291 rBV 89359 229244 2.69% 0.507% 2 11.670 717 722 745 rBV 2499627 6093458 71.61% 13.473% 3 15.277 1109 1115 1133 rBV 3754630 8072392 94.87% 17.848% 4 20.556 1683 1690 1705 rBV 3835817 8509314 100.00% 18.814% 5 24.981 2165 2172 2183 rBV2 3486280 7967747 93.64% 17.617%
6 25.119 2183 2187 2193 rVB 34468 90690 1.07% 0.201% 7 30.048 2719 2724 2730 rBV 239937 492583 5.79% 1.089% 8 33.014 3040 3047 3064 rBV2 2512805 5981064 70.29% 13.224% 9 35.566 3319 3325 3344 rBV 1106928 3090782 36.32% 6.834% 10 37.108 3484 3493 3510 rBV2 1595844 4701026 55.25% 10.394%
Sum of corrected areas: 45228300
28861.D GCMS1126.M Tue Dec 11 16:03:30 2001
NYC-WTC_000035750
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NYC-WTC_000035755
Lab report noting bis(2-Ethylhexyl) Sebacate detection and potential laboratory contamination in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035717
Laboratory notes identifying potential laboratory contamination by specific esters in sample AD28899.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035990
Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in sample AD29028 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035727
Laboratory notes stating the GCMS scan of sample AD28897 revealed no unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035909
Lab notes for sample AD29024 indicate detection of bis(2-Ethylhexyl)phthalate and no unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035843
Lab notes for sample AD29190 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036000
Analysis comments for sample AD29089 reporting no unusual compounds in GCMS scan but noting one compound recovery above acceptance range in LCS Standard.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035967
Laboratory report documenting GCMS scan results for sample AD29138 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035505
Gas chromatography-mass spectrometry analysis results for sample AD28859 showing bis(2-Ethylhexyl)phthalate presence at 0.81 ug/L with quality control notes on LCS standard recover
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036425
Laboratory report documenting GCMS analysis of sample AD29457 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033874
Laboratory report detailing GCMS scan results and recovery rates for environmental sample AD28147 analyzed in December 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019070
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30115 conducted on January 9, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000035662
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035663
Fragmented document containing method 508 data and sample IDs processed by GCMS in late 2001.
Filed in the same folder
NYC-WTC_000035664
Laboratory data sheet recording GCMS Method 508 analysis of a blank sample for nitrosamines and chlorinated compounds.
Filed in the same folder
NYC-WTC_000035674
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035678
Document containing calculated reference values for various organic compounds analyzed by GCMS.
Filed in the same folder