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Document / 11 pages

GCMS analysis comments, sample AD28970, Dec 2001

Machine-extracted title · confidence 90%

Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.

NYC-WTC_000035651–000035661

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\DEC0 701\28970.D Vial: 15 Acq On 8 Dec 2001 4:35 am Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 310 rBV 496460 1288659 17.34% 3.328% 2 11.349 683 687 692 rBV 50220 117627 1.58% 0.304% 3 11.431 692 696 709 rVB 52775 156645 2.11% 0.405% 4 11.670 716 722 740 rBV 2179355 5255603 70.72% 13.574% 5 15.278 1109 1115 1133 rBV 3177627 6752042 90.86% 17.438%

6 20.557 1683 1690 1704 rBV 3375982 7431219 100.00% 19.192% 7 24.972 2165 2171 2182 rBV2 3058513 7061550 95.03% 18.238% 8 25.119 2184 2187 2195 rVB 31182 80937 1.09% 0.209% 9 30.049 2719 2724 2732 rVB 495511 1048101 14.10% 2.707% 10 33.014 3040 3047 3066 rBV2 2266115 5429124 73.06% 14.022%

11 33.290 3072 3077 3093 rVB 64167 190266 2.56% 0.491% 12 37.100 3485 3492 3513 rBV2 1327686 3907640 52.58% 10.092%

Sum of corrected areas: 38719413

28970.D GCMS1126.M Thu Dec 13 10:29:28 2001

NYC-WTC_000035656

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NYC-WTC_000035656Source: NYC Law Department, mirrored locally

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