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GCMS analysis results sample AD29298, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29298 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036391–000036402

Folder label: “GCMS X 12/5/01 A 12/12/01

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Scanned page image, NYC-WTC_000036396
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC1201\29298.D Vial: 25 Acq On 13 Dec 2001 2:23 am Operator: 209 GALOS Sample gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 274 279 291 rBV 287381 784126 11.05% 2.144% 2 7.731 291 293 311 rVB2 32678 139740 1.97% 0.382% 3 11.339 682 686 691 rBV 107442 236961 3.34% 0.648% 4 11.422 691 695 710 rVB 112248 318435 4.49% 0.871% 5 11.670 715 722 74 8 rW 2106098 5372655 75.69% 14.689%

6 15.277 1109 1115 1133 rBV 3014685 6651487 93.70% 18.186% 7 20.556 1683 1690 1704 rBV 3110803 7098532 100.00% 19.408% 8 24.972 2165 2171 2184 rBV2 2990297 6616515 93.21% 18.090% 9 25.119 2184 2187 2201 rVB 26691 99877 1.41% 0.273% 10 30.049 2719 2724 2736 rVB 365996 737466 10.39% 2.016%

11 33.005 3039 3046 3065 rBV2 2051125 4835360 68.12% 13.220% 12 37.099 3484 3492 3514 rBV 1291310 3684160 51.90% 10.073%

Sum of corrected areas: 36575314

29298.D GCMS1126.M Fri Dec 21 12:20:37 2001

NYC-WTC_000036396

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NYC-WTC_000036396Source: NYC Law Department, mirrored locally

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