Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036278–000036288Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
Data File C:\HPCHEM\l\DATA\DEC1001\29455.D Vial: 6 Acq On 12 Dec 2001 4:37 am Operator: 209 GALOS Sample gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.594 273 278 304 rBV 551254 1359240 16.37% 3.112% 2 11.340 682 686 691 rBV 116279 255704 3.08% 0.585% 3 11.413 691 694 715 rVB 117776 346224 4.17% 0.793% 4 11.670 715 722 746 rBV 2624026 6130474 73.85% 14.034% 5 15.278 1109 1115 1133 rBV 3410198 7673806 92.44% 17.567%
6 20.557 1682 1690 1700 rBV 3707135 8301767 100.00% 19.005% 7 24.972 2164 2171 2184 rBV2 3532279 7791622 93.85% 17.837% 8 25.119 2184 2187 2199 rVB 32839 102210 1.23% 0.234% 9 26.983 2385 2390 2398 rBV 46045 102098 1.23% 0.234% 10 30.049 2718 2724 2731 rBV 521389 1062375 12.80% 2.432%
11 33.005 3039 3046 3064 rBV2 2491864 5864944 70.65% 13.426% 12 37.100 3484 3492 3513 rBV2 1633097 4691517 56.51% 10.740%
Sum of corrected areas: 43681981
29455.D GCMS1126.M Wed Dec 19 12:59:11 2001
NYC-WTC_000036283
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NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 1.000
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036447
Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder