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GCMS analysis comments, sample AD28859, December 2001

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry analysis results for sample AD28859 showing bis(2-Ethylhexyl)phthalate presence at 0.81 ug/L with quality control notes on LCS standard recover

NYC-WTC_000035505–000035513

Folder label: “GCMS X 11/27/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\28859.D Vial: 31 Acq On 7 Dec 2001 4:57 am Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.675 716 722 745 rBV 2284104 5765006 72.23% 14.033% 2 15.274 1108 1114 1132 rBV 3425141 7546216 94.55% 18.368% 3 20.552 1682 1689 1706 rBV 3670448 7981152 100.00% 19.427% 4 24.977 2164 2171 2182 rBV2 3513395 .7631298 95.62% 18.575% 5 25.124 2182 2187 2196 rVB 32984 100407 1.26% 0.244%

6 28.805 2583 2588 2600 rVB 197767 377544 4.73% 0.919% 7 30.054 2718 2724 2730 rBV 445568 944876 11.84% 2.300% 8 33.010 3039 3046 3066 rBV2 2414937 5770453 72.30% 14.046% 9 33.285 3071 3076 3092 rVB 112772 309529 3.88% 0.753% 10 37.104 3483 3492 3508 rBV2 1562420 4656145 58.34% 11.334%

Sum of corrected areas: 41082626

28859.D GCMS1126.M Wed Dec 12 11:38:14 2001

NYC-WTC_000035510

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NYC-WTC_000035510Source: NYC Law Department, mirrored locally

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