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GCMS analysis comments for sample AD28759, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report noting detection of Di-n-butylphthalate in a WTC environmental sample.

NYC-WTC_000035330–000035337

Folder label: “GCMS X 11/26/01 A 12/6/01

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Scanned page image, NYC-WTC_000035335
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0501\28760.D Vial: 13 Acq On 6 Dec 2001 12:20 am Operator: 209 GALOS Sample 11/26 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.715 721 727 744 rBV 1650937 4415621 73.81% 15.412% 2 15.314 1113 1119 1138 rBV 2722093 5813555 97.18% 20.291% 3 20.583 1687 1693 1707 rBV 2696890 5982485 100.00% 20.881% 4 25.008 2168 2175 2187 rBV2 2414662 5439013 90.92% 18.984% 5 25.155 2187 2191 2201 rVB 19844 69324 1.16% 0.242%

6 27.009 2389 2393 2401 rBV 34811 74325 1.24% 0.259% 7 30.076 2722 2727 2738 rVB 214350 437813 7.32% 1.528% 8 33.032 3043 3049 3067 rBV2 1556681 3716203 62.12% 12.971% 9 37.126 3488 3495 3517 rBV2 952126 2702517 45.17% 9.433%

Sum of corrected areas: 28650856

28760.D GCMS1126.M Fri Dec 07 17:03:09 2001

NYC-WTC_000035335

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NYC-WTC_000035335Source: NYC Law Department, mirrored locally

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