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GCMS analysis comments for sample AD28759, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting detection of Di-n-butylphthalate in a WTC environmental sample.

NYC-WTC_000035322–000035329

Folder label: “GCMS X 11/26/01 A 12/6/01

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Scanned page image, NYC-WTC_000035327
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0501\28759. D Vial: 14 Acq On 6 Dec 2001 1:18 am Operator: 209 GALOS Sample 11/26 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.715 721 727 746 rBV 1544819 4177866 72.18% 14.962% 2 15.314 1113 1119 1137 rBV 2573968 5489115 94.84% 19.658% 3 20.583 1687 1693 1709 rBV 2651882 5787739 100.00% 20.727% 4 25.008 2168 2175 2187 rBV2 2342024 5227382 90.32% 18.720% 5 25.155 2187 2191 2201 rVB 19254 64999 1.12% 0.233%

6 27.010 2388 2393 2403 rBV 38816 83778 1.45% 0.300% 7 30.076 2722 2727 2735 rBV 273853 549089 9.49% 1.966% 8 33.032 3043 3049 3068 rBV2 1578423 3764071 65.04% 13.480% 9 37.126 3487 3495 3511 rBV2 971958 2779433 48.02% 9.954%

Sum of corrected areas: 27923472

28759.D GCMS1126.M Fri Dec 07 17:02:42 2001

NYC-WTC_000035327

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NYC-WTC_000035327Source: NYC Law Department, mirrored locally

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