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GCMS analysis comments, sample AD28856, Dec 2001

Machine-extracted title · confidence 95%

GCMS scan results for sample AD28856 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate.

NYC-WTC_000035481–000035488

Folder label: “GCMS X 11/27/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0601\28856.D Vial: 33 Acq On 7 Dec 2001 6:54 am Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.670 717 722 753 rBV 2064498 5690639 72.06% 14.099% 2 15.278 1109 1115 1132 rBV 3385751 7375345 93.39% 18.273% 3 20.556 1683 1690 1708 rBV 3633292 7897020 100.00% 19.566% 4 24.972 2165 2171 2182 rBV2 3261030 7510509 95.11% 18.608% 5 25.119 2182 2187 2196 rVB 32526 102015 1.29% 0.253%

6 30.049 2719 2724 2730 rBV 461972 963563 12.20% 2.387% 7 33.014 3037 3047 3061 rBV 2453367 5862875 .74.24% 14.526% 8 33.289 3072 3077 3085 rBV 84181 208961 2.65% 0.518% 9 37.108 3485 3493 3514 rBV2 1614553 4750277 60.15% 11.769%

Sum of corrected areas: 40361204

28856.D GCMS1126.M Wed Dec 12 11:36:33 2001

NYC-WTC_000035486

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NYC-WTC_000035486Source: NYC Law Department, mirrored locally

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