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GCMS analysis comments, sample AD28855, Dec 2001

Machine-extracted title · confidence 95%

GCMS scan results for sample AD28855 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate and noting low pH.

NYC-WTC_000035473–000035480

Folder label: “GCMS X 11/27/01 A 12/7/01

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Scanned page image, NYC-WTC_000035478
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\DECO 601\28855.D Vial: 34 Acq On 7 Dec 2001 7:53 am Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.675 716 722 741 rBV 2485561 6104420 71.14% 14.448% 2 15.274 1108 1114 1132 rBV 3697859 8050465 93.82% 19.054% 3 20.553 1682 1689 1705 rBV 3810550 8581063 100.00% 20.310% 4 24.978 2164 2171 2182 rBV2 3576966 7978685 92.98% 18.884% 5 25.115 2183 2186 2193 rVB 35050 90816 1.06% 0.215%

6 30.054 2718 2724 2733 rVB 469477 1005372 11.72% 2.380% 7 33.010 3038 3046 3063 rBV2 2373679 5806747 67.67% 13.744% 8 33.295 3071 3077 3087 rBV 46339 129161 1.51% 0.306% 9 37.105 3483 3492 3508 rBV2 1515220 4503455 52.48% 10.659%

Sum of corrected areas: 42250184

28855.D GCMS1126.M Wed Dec 12 11:35:35 2001

NYC-WTC_000035478

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NYC-WTC_000035478Source: NYC Law Department, mirrored locally

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