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Document / 8 pages

GCMS analysis comments for sample AD28758, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in a WTC environmental sample.

NYC-WTC_000035314–000035321

Folder label: “GCMS X 11/26/01 A 12/6/01

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Scanned page image, NYC-WTC_000035319
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 501\28758.D Vial: 15 Acq On 6 Dec 2001 2:17 am Operator: 209 GALOS Sample 11/26 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.716 721 727 744 rBV 2239053 5731471 72.75% 14.883% 2 15.315 1113 1119 1138 rBV 3531825 7453570 94.61% 19.355% 3 20.593 1687 1694 1718 rBV 3389057 7878251 100.00% 20.458% 4 25.009 2168 2175 2187 rBV2 3341517 7260673 92.16% 18.854% 5 25.156 2187 2191 2203 rVB 31084 94597 1.20% 0.246%

6 30.077 2722 2727 2737 rVB 312461 616872 7.83% 1.602% 7 33.042 3042 3050 3068 rBV2 2209768 5312117 67.43% 13.794% 8 33.317 3075 3080 3088 rVB 37764 92473 1.17% 0.240% 9 37.136 3487 3496 3513 rBV2 1408219 4070022 51.66% 10.569%

Sum of corrected areas: 38510046

28758.D GCMS1126.M Fri Dec 07 17:02:14 2001

NYC-WTC_000035319

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NYC-WTC_000035319Source: NYC Law Department, mirrored locally

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