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GCMS analysis results for sample AD29962, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report documenting analysis of sample AD29962 conducted on January 28, 2002.

NYC-WTC_000037327–000037338

Folder label: “GCMS X 12/11/01 A 12/18/01

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Scanned page image, NYC-WTC_000037332
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1801\30011.D Vial: 14 Acq On 19 Dec 2001 4:47 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.598 274 278 290 rBV 296293 853569 13.87% 2.781% 2 7.736 290 293 315 rVB 55831 248006 4.03% 0.808% 3 11.362 683 688 692 rBV 31007 77848 1.26% 0.254% 4 11.436 692 696 7 03 rW2 27882 83075 1.35% 0.271% 5 11.674 716 722 750 rBV 1487377 4488616 72.93% 14.624%

6 15.273 1109 1114 1132 rBV 2346072 5560963 90.36% 18.118% 7 20.552 1683 1689 1712 rBV 2843952 6154356 100.00% 20.052% 8 24.977 2164 2171 2183 rBV2 2297135 5436362 88.33% 17.712% 9 30.053 2718 2724 2736 rBV 336160 678341 11.02% 2.210% 10 33.009 3039 3046 3065 rBV2 1647814 4030180 65.48% 13.131%

11 37.104 3485 3492 3512 rBV 1055697 3081374 50.07% 10.039%

Sum of corrected areas: 30692690

30011.D GCMS1126.M Tue Jan 15 15:30:40 2002

NYC-WTC_000037332

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NYC-WTC_000037332Source: NYC Law Department, mirrored locally

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