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GCMS analysis results for sample AD303B5, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.

NYC-WTC_000017782–000017795

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30355.D Vial: 7 Acq On : 27 Dec 2001 5:59 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan. TY height area % max. total

1 7.619 275 280 292 rBV 363368 1047101 14.75% 2.955% 2 11.456 694 698 712 rVB 24314 112940 1.59% 0.319% 3 11.677 717 722 749 rBV 1884802 5244127 73.90% 14.797% 4 14.311 1003 1009 1015 rBV 111375 238619 3.36% 0.673% 5 15.275 1109 1114 1135 rBV 2481611 6396137 90.13% 18.048%

6 17.451 1345 1351 1361 rVB2 167775 346263 4.88% 0.977% 7 20.278 1653 1659 1665 rBV 113822 240423 3.39% 0.678% 8 20.563 1683 1690 1710 rBV 2852313 7096689 100.00% 20.025% 9 22.785 1927 1932 1937 rBV 77519 167134 2.36% 0.472%' 10 24.979 2163 2171 2204 rBV2 2278240 6501252 91.61% 18.344%

11 26.888 2373 2379 2386 rVB 37021 80126 1.13% 0.226% 12 27.017 2386 2393 2405 rBV 45769 141009 1.99% 0.398% 13 30.065 2718 2725 2735 rBV 365217 825350 11.63% 2.329% 14 33.021 3039 3047 3068 rBV2 1479857 4170817 58.77% 11.769% 15 37.115 3486 3493 3514 rBV2 828904 2831817 39.90% 7.990%

Sum of corrected areas: 35439804

30355.D GCMS1126.M Wed Jan 02 10:55:16 2002

NYC-WTC_000017787

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NYC-WTC_000017787Source: NYC Law Department, mirrored locally

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