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GCMS analysis results for sample AD30356, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30356 conducted on January 10, 2002.

NYC-WTC_000017770–000017781

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30356.D Vial: 21 Acq On : 28 Dec 2001 7:34 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF. Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.618 276 280 288 rBV 543247 1355477 15.19% 2.891% 2 7.719 288 291 313 rVB 404024 1267244 14.20% 2.703% 3 11.446 693 697 704 rW 32213 91921 1.03% 0.196% 4 11.675 717 722 746 rBV 2668277 6717821 75.30% 14.330% 5 14.310 1002 1009 1016 rBV 94196 204572 2.29% 0.436%

6 15.283 1109 1115 1133 rBV 3296829 8109000 90.89% 17.298% 7 17.450 1345 1351 1360 rBV 116132 242834 2.72% 0.518% 8 20.277 1652 1659 1666 rBV 76426 159487 1.79% 0.340% 9 20.562 1683 1690 1711 rBV 3685370 8921738 100.00% 19.031% 10 22.784 1926 1932 1937 rBV 50401 109938 1.23% 0.235%'

11 24.987 2163 2172 2185 rBV2 3066856 8181446 91.70% 17.452% 12 27.007 2387 2392 2404 rBV 53040 157060 1.76% 0.335% 13 30.064 2719 2725 2735 rBV 461894 1049562 11.76% 2.239% 14 33.020 3040 3047 3074 rBV2 2272201 6029008 67.58% 12.861% 15 37.114 3485 3493 3517 rBV 1337870 4282436 48.00% 9.135%

Sum of corrected areas: 46879544

30356.D GCMS1126.M Wed Jan 02 10:56:51 2002

NYC-WTC_000017775

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NYC-WTC_000017775Source: NYC Law Department, mirrored locally

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