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GCMS analysis results for sample AD28269, Nov 2001

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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.

NYC-WTC_000034180–000034197

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2901\28263.D Vial: 33 Acq On : 29 NOV 2001 6:28 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.649 279 284 296 rBV 41453 125255 1.75% 0.331% 2 11.560 706 710 720 rBV 55095 130387 1.82% 0.345% 3 11.698 720 725 745 rBV 2075964 5068516 70.80% 13.401% 4 15.305 1112 1118 1135 rBV 3173048 6843448 95.59% 18.094% 5 20.575 1686 1692 1715 rBV 3294588 7159080 100.00% 18.929%

6 25.000 2167 2174 2184 rBV2 2851477 6325646 88.36% 16.725% 7 30.067 2721 2726 2738 rBV 285375 544637 7.61% 1.440% 8 33.023 3042 3048 3064 rBV2 1778043 4102581 57.31% 10.847% 9 35.576 3318 3326 3335 rBV 43868 121810 1.70% 0.322% 10 36.723 3444 3451 3463 rBV 72465 242758 3.39% 0.642% 11 37.118 3486 3494 3512 rBV2 1056597 2966521 41.44% 7.844% 12 38.027 3584 3593 3610 rBV 103740 459637 6.42% 1.215% 13 39.596 3753 3764 3783 rBV2 130469 718488 10.04% 1.900% 14 41.534 3962 3975 4003 rBV2 134974 1004869 14.04% 2.657% 15 43.957 4224 4239 4267 rBV5 117394 1053745 14.72% 2.786% 16 47.042 4555 4575 4601 rBV5 84665 953735 13.32% 2.522%

Sum of corrected areas: 37821113 28263.D GCMS1126.M Fri NOV 30 13:41:16 2001

NYC-WTC_000034186

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NYC-WTC_000034186Source: NYC Law Department, mirrored locally

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