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GCMS comments for sample AD28149, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033765–000033779

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2 601\28159.D Vial: 21 Acq On : 27 Nov 2001 6:15 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 11.556 705 709 719 rBV 56622 125960 1.81% 0.356% 2 11.693 719 724 749 rW 2100805 4987163 71.56% 14.111% 3 15.301 1111 1117 1135 rBV 3145786 6635772 95.22% 18.776% 4 20.571 1685 1691 1712 rBV 3228491 6968923 100.00% 19.719% 5 24.996 2166 2173 2187 rBV2 2884414 6274760 90.04% 17.755% 6 30.072 2720 2726 2732 rBV 332243 668188 9.59% 1.891% 7 33.029 3041 3048 3065 rBV2 1896854 4298599 61.68% 12.163% 8 36.719 3443 3450 3459 rBV 37945 112576 1.62% 0.319% 9 37.123 3486 3494 3506 rBV 1276798 3534402 50.72% 10.001% 10 38.032 3583 3593 3603 rBV2 53516 204160 2.93% 0.578%

11 39.602 3755 3764 3775 rBV2 63866 292113 4.19% 0.827% 12 41.539 3962 3975 3989 rBV3 72500 447190 6.42% 1.265% 13 43.981 4226 4241 4258 rBV3 58368 437075 6.27% 1.237% 14 47.047 4557 4575 4596 rBV6 37439 354647 5.09% 1.003%

Sum of corrected areas: 35341528 28159.D GCMS1126.M Wed NOV 28 11:15:41 2001

NYC-WTC_000033770

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NYC-WTC_000033770Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28155, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.

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