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GCMS comments for sample AD28666, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.

NYC-WTC_000034830–000034843

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV2901\28666.D Vial: 35 Acq On : 29 NOV 2001 8:26 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.561 706 710 720 rBV 43913 101753 1.73% 0.344% 2 11.699 720 725 745 rBV 1683987 4170443 71.02% 14.104% 3 15.297 1112 1117 1136 rBV 2607668 5638190 96.01% 19.068% 4 20.576 1686 1692 1716 rBV 2718324 5872324 100.00% 19.859% 5 24.992 2167 2173 2186 rBV2 2350322 5098125 86.82% 17.241%

6 30.069 2721 2726 2735 rBV 279695 544359 9.27% 1.841% 7 33.025 3041 3048 3065 rBV2 1324973 3081461 52.47% 10.421% 8 36.724 3444 3451 3458 rBV 43265 126242 2.15% 0.427% 9 37.110 3486 3493 3511 rBV2 738172 2102601 35.81% 7.111% 10 38.019 3584 3592 3603 rBV2 67078 243146 4.14% 0.822%

11 39.598 3754 3764 3783 rBV 85741 407560 6.94% 1.378'% 12 41.535 3963 3975 3990 rBV4 109248 727317 12.39% 2.460% 13 43.968 4223 4240 4260 rBV2 97173 785222 13.37% 2.656% 14 47.034 4557 4574 4594 rBV2 69182 670666 11.42% 2.268%

Sum of corrected areas: 29569409

28666.D GCMS1126.M Fri NOV 30 16:21:51 2001

NYC-WTC_000034834

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NYC-WTC_000034834Source: NYC Law Department, mirrored locally

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