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Document / 11 pages

GCMS comments for sample AD28649, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.

NYC-WTC_000034808–000034818

Folder label: “GCMS X 11/23/01 A 11/29/01

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Scanned page image, NYC-WTC_000034812
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2901\28593.D Vial: 36 Acq On : 29 Nov 2001 9:24 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.768 293 297 305 rBV 20469 61621 1.01% 0.217% 2 11.559 707 710 720 rBV 43089 112871 1.85% 0.398% 3 11.697 720 725 747 rBV 1663378 4558765 74.65% 16.070% 4 15.305 1112 1118 1136 rBV 2757199 6004776 98.33% 21.167% 5 20.574 1686 1692 1716 rBV 2816318 6106490 100.00% 21.526% 6 24.990 2167 2173 2187 rBV2 2318330 5186884 84.94% 18.284% 7 30.067 2721 2726 2734 rBV 237922 466729 7.64% 1.645% 8 33.023 3041 3048 3064 rBV2 1355635 3108213 50.90% 10.957% 9 36.153 3371 3389 3391 rBV4 33945 172371 2.82% 0.608% 10 37.117 3485 3494 3508 rBV2 812847 2288676 37.48% 8.068% 11 41.359 3930 3956 3959 rBV6 25849 227048 3.72% 0.800% 12 47.877 4647 4666 4669 rBV6 9705 74037 1.21% 0.261%

Sum of corrected areas: 28368481 28593.D GCMS1126.M Fri Nov 30 16:18:46 2001

NYC-WTC_000034812

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NYC-WTC_000034812Source: NYC Law Department, mirrored locally

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