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GCMS comments for sample AD28159, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033752–000033764

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2601\28153.D Vial: 17 Acq On : 27 NOV 2001 2:21 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.557 705 709 719 rBV 61837 141264 1.93% 0.390% 2 11.694 719 724 745 rW 2244271 5307301 72.51% 14.662% 3 15.302 1111 1117 1135 rBV 3353598 7044650 96.24% 19.462% 4 20.572 1684 1691 1713 rBV 3413633 7319841 100.00% 20.222% 5 24.997 2166 2173 2186 rBV2 3096402 6651784 90.87% 18.377%

6 30.073 2720 2726 2733 rBV 431241 874430 11.95% 2 .416% 7 33.029 3041 3048 3064 rBV2 1974824 4528400 61.86% 12.510% 8 36.178 3381 3391 3415 rVB9 25249 246839 3.37% 0.682% 9 37.124 3486 3494 3516 rBV2 1268499 3564462 48.70% 9.847% 10 39.593 3753 3763 3774 rBV4 22351 104586 1.43% 0.289% 11 41.521 3965 3973 3994 rVB3 41509 283879 3.88% 0.784% 12 43.972 4229 4240 4253 rVB8 20016 129582 1.77% 0.358%

Sum of corrected areas: 36197018 28153.D GCMS1126.M Tue NOV 27 15:43:25 2001

NYC-WTC_000033757

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NYC-WTC_000033757Source: NYC Law Department, mirrored locally

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