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Document / 11 pages

GCMS comments for sample AD28666, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.

NYC-WTC_000034819–000034829

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2901\28649 .D Vial: 48 Acq On : 30 Nov 2001 9:38 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.621 277 281 313 rBV 286522 835922 13.50% 2.727% 2 11.560 706 710 719 rBV 47500 117026 1.89% 0.382% 3 11.697 719 725 746 rW 1700525 4469241 72.18% 14.578% 4 15.305 1112 1118 1135 rBV 2724046 5981446 96.60% 19.511% 5 20.575 1686 1692 1707 rBV 2927766 6191994 100.00% 20.197% 6 25.000 2167 2174 2186 rBV2 2420999 5575635 90.05% 18.187% 7 30.067 2721 2726 2732 rBV 319672 661811 10.69% 2.159% 8 33.023 3041 3048 3066 rBV2 1611084 3759404 60.71% 12.263% 9 37.118 3486 3494 3510 rBV2 960840 2742105 44.28% 8.944% 10 43.948 4228 4238 4259 rVB5 26387 183666 2.97% 0.599% 11 47.032 4559 4574 4575 rBV3 28188 139027 2.25% 0.453%

Sum of corrected areas: 30657277 28649.D GCMS1126.M Fri Nov 30 16:19:50 2001

NYC-WTC_000034823

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NYC-WTC_000034823Source: NYC Law Department, mirrored locally

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