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GCMS comments for sample AD28151, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28151 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033789–000033799

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2 601\28151.D Vial: 18 Acq On : 27 Nov 2001 3:19 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs ; 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 11.560 706 710 720 rBV 42832 98554 1.71% 0.375% 2 11.698 720 725 744 rBV 1668155 4196597 72.75% 15.983% 3 15.296 1112 1117 1137 rBV 2595157 5590625 96.91% 21.292% 4 20.575 1685 1692 1708 rBV 2717381 5768828 100.00% 21.970% 5 24.991 2167 2173 2186 IBV2 2288842 4950207 85.81% 18.853%

6 30.067 2721 2726 2734 rBV 260728 512039 8.88% 1.950% 7 33.023 3041 3048 3069 rBV2 1291236 2902167 50.31% 11.053% 8 37.118 3487 3494 3506 rBV 752011 2076837 36.00% 7.910% 9 39.587 3756 3763 3773 rVB6 15331 60783 1.05% 0.231% 10 43.957 4224 4239 4253 rBV7 13565 100563 1.74% 0.383%

Sum of corrected areas: 26257200

28151.D GCMS1126.M Wed Nov 28 07:56:22 2001

NYC-WTC_000033794

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NYC-WTC_000033794Source: NYC Law Department, mirrored locally

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