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GCMS comments for sample AD28157, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033800–000033815

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2601\28157.D Vial: 16 Acq On ; 27 Nov 2001 1:22 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise ; Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.563 706 710 719 rW 41686 102803 1.81% 0.343% 2 11.691 719 724 745 rBV 1623811 4152334 73.01% 13.863% 3 15.299 1111 1117 1135 rBV 2604178 5487091 96.48% 18.319% 4 20.569 1685 1691 1710 rBV 2588732 5687176 100.00% 18.987% 5 24.993 2167 2173 2187 rBV 2307772 4896342 86.09% 16.347%

6 30.070 2721 2726 2733 rBV 265009 522314 9.18% 1.744% 7 33.026 3041 3048 3067 rBV 1367167 3098082 54.47% 10.343% 8 35.578 3320 3326 3332 rBV2 40479 99702 1.75% 0.333% 9 36.726 3445 3451 3459 rBV 62264 189339 3.33% 0.632% 10 37.121 3486 3494 3511 rBV 858633 2421287 42.57% 8.084%

11 38.029 3584 3593 3609 rBV 109267 453735 7.98% 1.515% 12 39.599 3753 3764 3789 rBV2 120750 631710 11.11% 2.109% 13 41.546 3962 3976 4001 rBV 120941 838903 14.75% 2.801% 14 43.978 4224 4241 4264 rBV3 92208 776451 13.65% 2.592% 15 47.054 4557 4576 4600 rBV6 60825 595757 10.48% 1.989%

Sum of corrected areas: 29953026

28157.D GCMS1126.M Wed Nov 28 09:13:35 2001

NYC-WTC_000033805

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NYC-WTC_000033805Source: NYC Law Department, mirrored locally

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NYC-WTC_000033765

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NYC-WTC_000033834

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