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DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30710.D Vial: 48 Acq On : 30 Dec 2001 5:23 am Operator: 209 GALOS Sample . : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.613 276 280 311 rBV 395841 1254740 10.90% 1.985% 2 11.671 717 722 747 rBV 3322166 8845621 76.88% 13.994% 3 14.306 1003 1009 1018 rVB 360657 761049 6.61% 1.204% 4 15.279 1109 1115 1134 rBV 4525137 10911825 94.83% 17.263% 5 17.455 1345 1352 1361 rBV 741338 1591907 13.84% 2.518%

6 18.152 1422 1428 1436 rBV 58253 131070 1.14% 0.207% 7 20.273 1653 1659 1669 rBV 543426 1149231 9.99% 1.818% 8 20.557 1684 1690 1708 rBV 4661383 11347102 98.62% 17.951% 9 21.044 1738 1743 1764 rBV 84437 406312 3.53% 0.643% 10 22.788 1927 1933 1946 rBV 324528 678224 5.89% 1.073%

11 24.982 2163 2172 2204 rBV2 4199165 11506356 100.00% 18.203% 12 26.892 2373 2380 2389 rVB 124774 257627 2.24% 0.408% 13 28.654 2565 2572 2578 rBV 79781 171568 1.49% 0.271% 14 30.059 2720 2725 2735 rBV 410840 922074 8.01% 1.459% 15 30.252 2740 2746 2752 rVB 65753 150306 1.31% 0.238%

16 33.024 3041 3048 3070 rBV2 2982812 7920595 68.84% 12.531% 17 37.119 3486 3494 3519 rBV2 1626192 5204494 45.23% 8.234%

Sum of corrected areas: 63210101

30710.D GCMS1126.M Mon Jan 28 11:35:51 2002

NYC-WTC_000004284

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NYC-WTC_000004284Source: NYC Law Department, mirrored locally

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