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GCMS calibration results for sample AD28662, Dec 2001

Machine-extracted title · confidence 100%

Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.

NYC-WTC_000034958–000034970

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data'File : C:\HPCHEM\1\DATA\DEC0401\LB.D Vial: 3 Acq On : 4 Dec 2001 2:19 pm Operator: 209 GALOS Sample : 1b 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 11.574 707 711 721 rBV 47319 123261 1.89% 0.357% 2 11.711 721 726 738 rBV 1811435 4810209 73.62% 13.921% 3 14.337 1007 1012 1017 rBV 47750 91830 1.41% 0.266% 4 15.310 1113 1118 1136 rBV 2853306 6334134 96.94% 18.331% 5 17.476 1347 1354 1361 rVB 286854 545796 8.35% 1.580%

6 20.295 1655 1661 1668 rBV 269464 532586 8.15% 1.541% 7 20.589 1686 1693 1707 rBV 2970586 6534227 100.00% 18.910% 8 21.038 1737 1742 1754 rVB 165117 359481 5.50% 1.040% 9 22.810 1929 1935 1942 rVB 177279 345108 5.28% 0.999% 10 25.004 2165 2174 2188 rBV2 2676535 6100479 93.36% 17.655%

11 26.905 2373 2381 2386 rBV 65237 131223 2.01% 0.380% 12 28.667 2569 2573 2579 rVB 41366 84079 1.29% 0.243% 13 30.081 2722 2727 2734 rBV 223107 455598 6.97% 1.319% 14 30.265 2742 2747 2754 rVB 34804 72831 1.11% 0.211% 15 33.037 3042 3049 3068 rBV 1946904 4536178 69.42% 13.128%

16 37.131 3487 3495 3509 rBV2 1246033 3496983 53.52% 10.120%

Sum of corrected areas: 34554003 LB.D GCMS1126.M Thu Dec 06 14:40:45 2001

NYC-WTC_000034962

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NYC-WTC_000034962Source: NYC Law Department, mirrored locally

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