GCMS analysis comments for sample AD28688, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\28688.D Vial: 6 Acq On : 4 Dec 2001 5:15 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Hexene, 2-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 29.44 3.41 ug/1 681855 Chrysene-d12 33.04 Hit# of 5 Tentaylve ID MW MolForm CAS# Qual ------------------- ------------------------------------------------- 1 1-Hexene, 2-me 1- 98 C7H14 006094-02-6 27 2 Cyclobutane, ,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 3 1-Pentene, ,4-dimethyl- 98 C7H14 002213-32-3 27 4 Butyl hexad'ecanoate 312 C20H4002 000000-00-0 25 undance Scan 2657 (29.440 min): 28688.D (-) m z 56.00 100.00%

5000 41 73 257 129 239 7 1i5 143157171185199213 312 29.20 29.40 29.60 29.80 m z 57.00 49.81% -> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 thundance #1354: 1-Hexene, 2-methyl-

41 5000 29.20 29.40 29.60 29.80 27 70 m z 41.00 43.58% 98

n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 bundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl-

29.20 29.40 29.60 29.80 5000 m z 43.00 40.09%

27 70 97111125140 168 196 u u u i u i u u u ritz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63264: 1-Pentene, 2,4-dimethyl- 29.20 29.40 29.60 29.80 m z 55.00 30.05% 41 5000

27 70 98 I 1 1 1 1 1 1 1 11 1 1 1 1 u . 1 1 -> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

28688.D GCMS1126.M Thu Dec 06 13:23:08 2001 Page 2

NYC-WTC 000035033