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GCMS analysis comments for sample AD28688, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting di-n-butylphthalate detection and TurboVap contamination with recovery data for sample AD28688.

NYC-WTC_000035026–000035043

Folder label: “GCMS X 11/24/01 A 12/4/01

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Scanned page image, NYC-WTC_000035034
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\28688.D Vial: 6 Acq On 4 Dec 2001 5:15 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ***********************:r********************************************* Peak Number 3 Heptadecane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 29.55 0.70 ug/l 138894 Chrysene-d12 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qua].

1 Heptadecane 240 C17H36 000629-78-7 1' 2 Octadecane 254 C18H38 000593-45-3 3 Heneicosane 296 C21H44 000629-94-7 4 Hexadecane 226 C16H34 000544-76-3 undance Scan 2669 (29.550 min): 28688.D (-) m z 57 . 00 10 0 . 00%

71

5000 85

99 29.20 29.40 29.60 29.80 113127141155169183197 m/z 43.00 79.58% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 undance #71193: Heptadecane 5

4 71 5000 85 29.20 29.40 29.60 29.80 m/z 71.00 72.28% 113127141 155169 210 240 -> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 thundance #71560: Octadecane 43

71 29.20 29.40 29.60 29.80 5000 85 m/z 85.00 48.31%

99 113127141 169183197210 254 nlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 undance #42201: Heneicosane 29.20 29.40 29.60 29.80 71 - m/z 41.05 34.64% 85 5000

99 113127141155 268 29~; 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

28688.D GCMS1126.M Thu Dec 06 13:23:10 2001 Page 3

NYC-WTC 000035034

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NYC-WTC_000035034Source: NYC Law Department, mirrored locally

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