GCMS analysis sample AD26538, unknown compounds, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\26538.D Vial: 13 Acq On 6 Dec 2001 9:06 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1-Butanamine Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

10.33 0.46 ng/uL 128602 l,4-Dichiorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Butanamine 73 C4H11N 000109-73-9 9 2 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 9 3 Octane, 3,4-dimethyl- 142 C10H22 015869-92-8 9 4 2-NitroZl-propanol 105 C3H7NO3 _ 002902-96-7 9 Abundance Scan 599 (10.332 min): 26538.D (-) m/z 43.0,5 100.00% 43

5000 55 73 85 10.00 10.20 10.40 10.60 111 — — ll i । i . . i . i TT’T 1111.. ।.... j.... j. Tprr 1111111111111 m/z ( 39.48% m/z-> 10 20 30 40 50 60 70. 80 90 100 110 120 130 140 'Abundance #62539:1-Butanamine SO

1 । 5000 T11r T T 10.00 10.20 10.40 10.60 m/ z 59.00 38.82% 1154 THr

A 41 56 73 ■ i■■■•i ■ ■ ■ ■ i ■ ■'1111 ■'i•■ ■ ■ i • ■ “ i11111‘111111111111' I miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 (Abundance #637. Pyrrolidne, 3-methyl- 43 ! • • i ' ‘ 10.00 10.20 10.40 10.60 5000 m/z 57.10 37.03% 85 15 27 56 68 i . 1 | .... | . . TTT I I I I I .<> | > w . I I r I I I I I I I । I 1 11 | ■»। • ■ * * | 1 . . . j .... | .... J miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance i 43 #8107: Octane, 3,4-dimethyl- ' ' I * ' • ‘ I ‘ ' 10.00 10.20 10.40 10.60 —R i m/z 41. 10 34.98% 5000

Uy 57 85 27 71 - ’11113I — 113 142 1’——011—u—npunii A +A44—0A m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 10.00 10.20 10.40 10.60

26538.D NP112701.M Fri Dec 07 14:47:15 2001 Page 6

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