GCMS analysis sample AD26538, unknown compounds, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 601\26538.D Vial: 13 Acq On 6 Dec 2001 9:06 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 2-Pentanol, 4-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

10.54 0.43 ng/uL 119273 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 33 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 33 3 2-Pentanol, 4--methyl - 102 C6H140 000108-11-2 28 4 Hydroxyl arpine, O-hexyl- 117 C6H15NO 004665-68-3 12 Abundance * Scan 622 (10,543 min): 26538.D (-) m/ z 43710 100.00% f l> 43 _____

5000 85 39 57 69 10.20 10.40 10.60 10.80 miz-> 46... 461... i.... .................................. 36 | । I ‘ “ 11 ’'1 ‘ I “ “ J “ ' ‘ I “ “ I “ HIH 10 15 20 25 30 35 40 45 50 55 60 65 70 75 T’IT TH 80 85 90 95 m/z 45.05 77.54% Abundance #1773:2-Pentanol. 4-methyl- 45

5000 A,A,44—A,4, 4A-4-Pn 10.20 10.40 10.60 10.80 69 m/ z 31.26% 27 42 57 84 87 TTT tpmmp TOTTI—uaua miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547; 2-Pentanol, 4-methyl- I 45 1A A A _ A—AAA 10.20 10.40 10.60 10.80 5000 m/z 85.05 21.83% 27 69 ! “1 *!' ‘ “ I “ 1 ’ I 38 42 57 84 87 TDTTIITTTTIITT j.|lI..,.Il.।....।.1....j...I।. I..11 . . I | I I m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 — Abundance ’ #63546: 2-Pentanol, 4-methyl- • I • ‘ ‘ I * ’ 1 * H | 45 10.20 10,40 10.60 10.80 rn/z 44.05 17.14%

miz. 5000

10 19 15 20 25 30 35 27 31 57 42 TIPTgr— tpHnp • ’ I “ * p-rTTp-rrrfT Tm 40 45 50 55 60 65 70 75 80 69 84 87 85 90 95 0 10.20 10.40 10.60 10.80

26538.D NP112701.M Fri Dec 07 14:47:17 2001 Page 7

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