GCMS analysis sample AD26538, unknown compounds, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0601\26538.D Vial: 13 Acq On 6 Dec 2001 9:06 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Ethane, 1,1,2,2-tetrachloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

9.63 2.68 ng/uL 748252 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5 2 Ethane, l, l,2,2-tetrachloro- 166 C2H2C14 000079-34-5- 93 3 Ethane, l, 1,2-trichloro-2-fluoro- 150 C2H2C13F 000359-28-4 72 4 Ethane, 1,2,2-trichloro-1,1-difluor 168 C2HC13F2 000354-21-2 49 Abundance Scan 522 (9.626 mln): 26538.D (-) ‘ iiim/z 82.95 100.00% 83

5000

TITICCTCISITT6I2ttIr 37 47 61 73 95 131 9.20 9.40 9.60 9.80 10.00 miz-> TTIUTHmmgm -H 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 - --l 168 m/z 84.95 64.21% Abundance #13774: Ethane, 1,1,2,2-tetrachloro- 83

5000 . . । . . > . । , r, । । i i > । । । 9.20 9.40 9.60 9.80 10.00 95 m/z 94.9 13.15% | 35 47 131 168 miz-> 30 40 50 60 70 ’ 80 44+ T I I ’11’ i' ■ ■' i T i 11 90 100 110 120 130 140 150 160 170 Abundance #67919: Ethane, 1,1,2,2-tetrachioro- 83 11t11IIT ■ ■ . , ‘tr 1518 T IdT 9.20 9.40 9.60 9.80 10.00 5000 m/z 86.9, 9.86% 35 47 6 TILWTILTTLTLLmmT 96 131 ' I'' ‘ ’ i'1111' 168 Mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #9542: Ethane, 1,1,2-trichloro-2-fluoro- LA 83 9.20 9.40 9.60 9.80 10.00

L m/z 61.00 9.73% 5000 67 35 47 95 150 TTm — •1 ‘ i ■ • ■ ‘ | ‘11' i " 1 ■ i'1" i' Lu ,, ■1 'T1'11 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 9.20 9.40 9.60 9.80 10.00

26538.D NP112701.M Fri Dec 07 14:47:13 2001 Page 5

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